ขวดก้นกลม (round bottom flask)


 round_bottom_flask

ขวดก้นกลม (Round bottom flasks) รูปร่างขวดมีลักษณะก้นขวดกลม มีคอขวดอยู่ด้านบน จึงเรียกว่าขวดก้นกลม ใช้ในปฏิบัติการทางด้านเคมี และชีวเคมี เนื่องจากขวดก้นกลมต้องใช้ในสภาวะอุณหภูมิสูง และใส่สารเคมีหลากหลายชนิด จึงทำด้วยแก้วบอโรซิลิเกต คอขวดต้องมีอย่างน้อย 1 คอ อาจพบ 2 หรือ 3 คอ เพื่อใช้ประโยชน์อย่างอื่นร่วมด้วย เช่น คอหนึ่งใช้ต่อกับเครื่องควบแน่น (condenser) อีกคอหนึ่งใช้ต่อกับเทอร์โมมิเตอร์ (thermometer) ขนาดของขวดก้นกลมมีตั้งแต่ 5 มิลลิลิตร ถึง 5 ลิตร หรือมากกว่า การใช้งานขวดก้นกลม (Round bottom flasks) ใช้ในงานได้หลากหลายประเภท โดยปกติแล้วจะใช้ต้มหรือให้ความร้อน พบได้ในการกลั่นเพื่อแยกสารผสมออกจากกัน

Round bottom flasks (also called round-bottomed flasks and Erlenmeyer Bulbs) are types of flasks having spherical bottoms used as laboratory glassware, mostly for chemical or biochemical work. They are typically made of glass for chemical inertness; and in modern days, they are usually made of heat-resistant borosilicate glass. There is at least one tubular section known as the neck with an opening at the tip. Two or three-necked flasks are common as well. Round bottom flasks come in many sizes, from 5 mL to 5 L, with the sizes usually inscribed on the glass. In pilot plants even larger flasks are encountered.

 

The ends of the necks are usually conical (female) ground glass joints. These are standardized, and can accept any similarly-sized tapered (male) fittings. Standard Taper 24/40 is common for 250 mL or larger flasks, while smaller sizes such as 14 or 19 are used for smaller flasks.

 

Because of the round bottom, cork rings are needed to keep the round bottom flasks upright. When in use, round-bottom flasks are commonly held at the neck by clamps on a stand.

 

Applications

The round bottoms on these types of flasks allow more uniform heating and/or boiling of liquid. Thus, round-bottom flasks are used in a variety of applications where the contents are heated or boiled. Round-bottom flasks are usually used in distillation by chemists as distilling flasks and receiving flasks for the distillate (see distillation diagram). One-neck round-bottom flasks are used as the distilling flasks in rotary evaporators.

 

Round-bottom flasks are often used to contain chemical reactions run by chemists, especially for reflux set-ups and laboratory-scale synthesis. Boiling chips are often added in distilling flasks for distillations or boiling chemical reactions to allow a nucleation site for gradual boiling. This nucleation avoids a sudden boiling surge where the contents may overflow from the boiling flask. Stirring bars or other stirring devices suited for round-bottom flasks are sometimes used. For a reflux set-up, a condenser is typically attached to the middle or only neck of the flask being used. Additional necks on a flask could allow a thermometer or a mechanical stirrer to be inserted into the flask contents. The additional necks can also allow a dropping funnel to be attached to let reactants slowly drip in.

 

Special electrically powered heating mantles are available in various sizes into which the bottoms of round-bottom flasks can fit so that the contents of a flask can be heated for distillation, chemical reactions, boiling, etc. Heating can also be accomplished by submerging the bottom of the flask into a heat bath, water bath, or sand bath. Similarly cooling can be accomplished by partial submerging into a cooling bath, filled with e.g. cold water, ice, eutectic ice/salt mixtures, dry ice/solvent mixtures, or liquid nitrogen 

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